High-Throughput Hydrothermal Synthesis Platform

High-Throughput Hydrothermal Synthesis Platform

High-Throughput Hydrothermal Synthesis Platform

This platform is engineered for the synthesis of molecular sieve catalysts and can be adapted to various reaction scenarios in molecular sieve preparation. It primarily handles hydrothermal synthesis and ion exchange reactions, while also supporting auxiliary processes like molecular sieve crystallization and modification. The platform can prepare commonly used zeolite catalysts such as ZSM-5, Y-type, SAPO series, and others, fulfilling requirements for catalytic cracking, isomerization, alkylation, denitration and desulfurization, adsorption, separation, and otherrelated catalytic applications. Addressing several key challenges in molecular sieve synthesis, the platform features a high-throughput parallel design that significantly boosts efficiency. It offers full automation with precise parameter control throughout the entire closed-loop process, enabling a smooth transition from research and development to mass production. With enhanced safety features and strong adaptability, it comprehensively accelerates both R&D and industrialization efforts.

Features

More Efficient
Adopts high-throughput parallel design for multi-batch, multi-crystal-form and multi-formula molecular sieve synthesis. Its efficiency is 6–12 times higher than traditional methods, drastically shortening R&D and preparation cycles.
More Precise
Full-process automation precisely controls key synthesis parameters and eliminates manual operation errors, ensuring consistent crystal forms, pore sizes and catalytic performance of molecular sieves across all batches.
Easy Scale-Up
Supports seamless transition from lab-scale to pilot-scale experiments with parameters compatible with industrial standards. Complete experimental data recording reduces the cost and difficulty of converting lab achievements to mass production.
Safer
Automated operations isolate operators from hazardous materials and harsh working conditions, paired with intelligent protection systems for enhanced safety. Remote control is supported to simplify operation and lower operator skill requirements.
More Flexible
Compatible with diverse molecular sieve synthesis requirements with freely configurable process parameters. It can independently complete single-process experiments or realize full-process automated synthesis.

Specifications

Module	Item	Specifications
Solid Dosing Unit	Supported Solid Types	20 types
	Single Vial Solid Storage Capacity	≤5 g
	Feeding Method	Negative Pressure Suction Weighing Method
	Single Sample Solid Addition Range	0.1–500 mg
	Matching Grippers	Vial/tube gripper, cap-tightening gripper, negative pressure suction feeding connector
	Operation Requirement	Replace feeding connector for different solids; add the same material in batches
Liquid Dosing Unit	Organic Solvents	5 types (including ultra-dry reagents); single vial storage volume: 250 mL; dosing volume: 0.1–15 mL; liquid transfer pipetting method
	Mineralizers	5 types; single vial storage volume: 50 mL; concentration range: 1 mM to pure acid (e.g. 14 M concentrated nitric acid, 12 M concentrated hydrochloric acid, 99.5% formic acid); dosing volume: 10 μL–5 mL; liquid transfer pipetting method
	Detergents / Washing Solvents	5 types; single vial storage volume: 500 mL; single consumption volume: 5–50 mL; pump liquid delivery method, supports switching between different detergents
	Pipette Tip Specifications	200 μL, 1000 μL
	Operation Requirements	Replace pipette tips for different liquids; add the same reagent in batches
Stirring & Ultrasonic Unit	Stirring Speed	0–1200 rad/min
	Heating Temperature under Stirring	≤300°C
	Single Batch Stirring Throughput	Simultaneously process 30–50 pieces of 20 mL glass vials / centrifuge tube liners
	Ultrasonic Power	400 W
	Ultrasonic Frequency	3 adjustable gears: 40 / 80 / 120 kHz
	Single Batch Ultrasonic Throughput	Simultaneously process 30–50 pieces of 20 mL glass vials / centrifuge tube liners
	Matching Grippers	Vial/tube gripper, cap-tightening gripper, tray gripper
Autonomous Reactor Disassembly & Drying Unit	Reactor Specification	Volume: 20–25 mL, matched with 20–25 mL PTFE centrifuge-tube liners (compatible with centrifuges)
	Single Batch Reaction Station Capacity	≥50 units
	Reactor Operation Module	Automatic capping & uncapping unit, compatible with AGV automatic material transfer
	Oven Temperature Range	RT-350°C
	Oven Temperature Accuracy	0.1°C
	Oven Control Functions	Programmable temperature ramp-up
	Oven Configuration	2 units required; each oven holds 50 reactors or 100 pcs of 20 mL vials
	Marking Function	Supports serial numbering or inkjet coding marking for reactors/vials
	Transfer Mode	AGV automatically transports centrifuge tube racks, hydrothermal reactors and ovens
Centrifugal Washing Unit	Centrifuge Stations	6–8 stations
	Compatible Centrifuge Tubes	50 mL (matching 20–25 mL reactor liners)
	Minimum Centrifuge Rotational Speed	≥11000 rpm
	Standard Washing Cycles	4 cycles (adjustable per experimental requirements)
	Washing Mode	Centrifugal washing; optional filtration washing with supporting waste liquid collection stations
	Matching Grippers	Vial/tube gripper, tray gripper
	Parallel Processing Capacity	Operates simultaneously with reactor heating process
Scraping & Collection Unit	Scraping Mode	Automatic scraping via robotic arm scraper (for solid wall detachment)
	Material Collection Mode	Negative pressure suction transfers solids to hopper then to vials; manual collection available upon negative pressure failure
	Collection Vessel	20 mL crimp vial
	Sealing Method	Automatic capping & sealing
	Marking Function	Supports serial numbering or inkjet coding for crimp vials
	Matching Grippers	Vial/tube gripper, capping gripper, scraper gripper, negative pressure suction gripper

Tel：400-1028-599

Europe:

Yanghong@osskj.com

Other Regions:

oushisheng@osskj.com

Address：

Building 9, Plaza 7, Dijing Road, Haidian District, Beijing, China